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Beilstein J. Org. Chem. 2022, 18, 1338–1345, doi:10.3762/bjoc.18.139
Graphical Abstract
Scheme 1: Synthesis of bis(chlorophenyl)acetylenes 3.
Scheme 2: Synthesis of 1,2,3-tris(chlorophenyl)cyclopropenylium bromides 5 and tributyl(1,2,3-tris(chlorophen...
Figure 1: ORTEP representations for cations 5c (a) and 6c (b) at the 50% probability level. Bromide anion and...
Scheme 3: Synthesis of 3,4,5-tris(chlorophenyl)-1,2-diphosphacyclopentadienides 7 and 3,4,5-tris(chlorophenyl...
Figure 2: Considered conformations of 8b-I and 8b-II.
Figure 3: Top: experimental UV–vis spectra of 8с (black) and 8b (red). Bottom: broadened calculated UV–vis sp...
Figure 4: Frontier orbitals of 8b-II contributing to absorption bands at about 380 nm.
Figure 5: Cyclic voltammograms of 3,4,5-triaryl-1,2-diphosphaferrocenes 8b and 8c in CH3CN on glassy carbon e...